The identification of synthetic cannabinoids surface coated on herbal substrates using solid-state nuclear magnetic resonance spectroscopy

N. K. Burns; A. G. Theakstone; H. Zhu; L. A. O'Dell; J. R. Pearson; T. D. Ashton; F. M. Pfeffer; X. A. Conlan

doi:10.1016/j.aca.2019.12.051

The identification of synthetic cannabinoids surface coated on herbal substrates using solid-state nuclear magnetic resonance spectroscopy

N. K. Burns, A. G. Theakstone, H. Zhu, L. A. O'Dell, J. R. Pearson, T. D. Ashton, F. M. Pfeffer, X. A. Conlan^*

^*Corresponding author for this work

Research output: Contribution to journal › Article › peer-review

10 Scopus citations

Abstract

Solid-state ¹³C and ¹⁹F NMR spectroscopy offers a non-destructive, highly selective protocol for the identification of forensically relevant synthetic cannabinoids on herbal substrates. Using this technique, well resolved ¹³C spectra were obtained that readily enabled structural identification; in some instances complemented by ¹⁹F spectral data. The approach described has potential for related applications such as the direct detection of pesticides on plants.

Original language	English
Pages (from-to)	105-109
Number of pages	5
Journal	Analytica Chimica Acta
Volume	1104
DOIs	https://doi.org/10.1016/j.aca.2019.12.051
State	Published - 1 Apr 2020
Externally published	Yes

Keywords

Herbal substrates
Solid state nuclear magnetic resonance spectroscopy
Surface coating
Synthetic cannabinoids

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10.1016/j.aca.2019.12.051

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title = "The identification of synthetic cannabinoids surface coated on herbal substrates using solid-state nuclear magnetic resonance spectroscopy",

abstract = "Solid-state 13C and 19F NMR spectroscopy offers a non-destructive, highly selective protocol for the identification of forensically relevant synthetic cannabinoids on herbal substrates. Using this technique, well resolved 13C spectra were obtained that readily enabled structural identification; in some instances complemented by 19F spectral data. The approach described has potential for related applications such as the direct detection of pesticides on plants.",

keywords = "Herbal substrates, Solid state nuclear magnetic resonance spectroscopy, Surface coating, Synthetic cannabinoids",

author = "Burns, {N. K.} and Theakstone, {A. G.} and H. Zhu and O'Dell, {L. A.} and Pearson, {J. R.} and Ashton, {T. D.} and Pfeffer, {F. M.} and Conlan, {X. A.}",

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doi = "10.1016/j.aca.2019.12.051",

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AU - Burns, N. K.

AU - Theakstone, A. G.

AU - Zhu, H.

AU - O'Dell, L. A.

AU - Pearson, J. R.

AU - Ashton, T. D.

AU - Pfeffer, F. M.

AU - Conlan, X. A.

PY - 2020/4/1

Y1 - 2020/4/1

N2 - Solid-state 13C and 19F NMR spectroscopy offers a non-destructive, highly selective protocol for the identification of forensically relevant synthetic cannabinoids on herbal substrates. Using this technique, well resolved 13C spectra were obtained that readily enabled structural identification; in some instances complemented by 19F spectral data. The approach described has potential for related applications such as the direct detection of pesticides on plants.

AB - Solid-state 13C and 19F NMR spectroscopy offers a non-destructive, highly selective protocol for the identification of forensically relevant synthetic cannabinoids on herbal substrates. Using this technique, well resolved 13C spectra were obtained that readily enabled structural identification; in some instances complemented by 19F spectral data. The approach described has potential for related applications such as the direct detection of pesticides on plants.

KW - Herbal substrates

KW - Solid state nuclear magnetic resonance spectroscopy

KW - Surface coating

KW - Synthetic cannabinoids

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DO - 10.1016/j.aca.2019.12.051

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EP - 109

JO - Analytica Chimica Acta

JF - Analytica Chimica Acta

ER -

The identification of synthetic cannabinoids surface coated on herbal substrates using solid-state nuclear magnetic resonance spectroscopy

Abstract

Keywords

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