Electrodeposited spruce leaf-like structured copper bismuth oxide electrode for supercapacitor application

Ahmed AL-Osta; Bushra Saleh Samer; Umesh T. Nakate; Vijaykumar V. Jadhav; Rajaram S. Mane

doi:10.1016/j.mee.2020.111359

Electrodeposited spruce leaf-like structured copper bismuth oxide electrode for supercapacitor application

Ahmed AL-Osta^*, Bushra Saleh Samer, Umesh T. Nakate, Vijaykumar V. Jadhav, Rajaram S. Mane

^*Corresponding author for this work

Research output: Contribution to journal › Article › peer-review

17 Scopus citations

Abstract

Novel spruce leaf-like copper bismuth oxide (CuBi₂O₄) microstructured films have been deposited on stainless steel (SS) substrate by using a simple and cost-effective electrodeposition chemical route. The morphology of CuBi₂O₄ was studied using field emission scanning electron microscopy (FESEM) whereas X-ray diffraction (XRD) spectra recorded for phase confirmation. The spruce leaf-like architecture composed of nanoparticles was evidenced for the obtained CuBi₂O₄ material. The supercapacitor performance for prepared CuBi₂O₄ electrode calcined at 200, 300, 400, 500 °C temperatures were investigated. The cyclic-voltammetry and charge-discharge studies were carried out at different scan rates and current densities respectively. The highest specific capacitance 484 F/g was noted for CuBi₂O₄ electrode calcined at 500 °C at 10 mV/ s scan rate via cyclic-voltammetry analysis in 1 M NaOH electrolyte. The specific capacitance of 540.9 F/g was estimated from charge-discharge analysis at 10 mA/cm² current density. The energy density of 146.8 Wh/Kg and power density 1555.5 W/Kg for optimized CuBi₂O₄ electrode at 10 mA/cm² current density. The electrochemical impedance spectroscopy studies were also performed. The nanostructured CuBi₂O₄ material has exhibited supercapacitive properties for energy storage applications.

Original language	English
Article number	111359
Journal	Microelectronic Engineering
Volume	229
DOIs	https://doi.org/10.1016/j.mee.2020.111359
State	Published - 15 May 2020
Externally published	Yes

Keywords

Calcination effect
Charge transport kinetics
Copper bismuth oxide
Electrochemical measurements
Specific capacitance
Spruce leaf-like nanostructure

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10.1016/j.mee.2020.111359

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title = "Electrodeposited spruce leaf-like structured copper bismuth oxide electrode for supercapacitor application",

abstract = "Novel spruce leaf-like copper bismuth oxide (CuBi2O4) microstructured films have been deposited on stainless steel (SS) substrate by using a simple and cost-effective electrodeposition chemical route. The morphology of CuBi2O4 was studied using field emission scanning electron microscopy (FESEM) whereas X-ray diffraction (XRD) spectra recorded for phase confirmation. The spruce leaf-like architecture composed of nanoparticles was evidenced for the obtained CuBi2O4 material. The supercapacitor performance for prepared CuBi2O4 electrode calcined at 200, 300, 400, 500 °C temperatures were investigated. The cyclic-voltammetry and charge-discharge studies were carried out at different scan rates and current densities respectively. The highest specific capacitance 484 F/g was noted for CuBi2O4 electrode calcined at 500 °C at 10 mV/ s scan rate via cyclic-voltammetry analysis in 1 M NaOH electrolyte. The specific capacitance of 540.9 F/g was estimated from charge-discharge analysis at 10 mA/cm2 current density. The energy density of 146.8 Wh/Kg and power density 1555.5 W/Kg for optimized CuBi2O4 electrode at 10 mA/cm2 current density. The electrochemical impedance spectroscopy studies were also performed. The nanostructured CuBi2O4 material has exhibited supercapacitive properties for energy storage applications.",

keywords = "Calcination effect, Charge transport kinetics, Copper bismuth oxide, Electrochemical measurements, Specific capacitance, Spruce leaf-like nanostructure",

author = "Ahmed AL-Osta and Samer, {Bushra Saleh} and Nakate, {Umesh T.} and Jadhav, {Vijaykumar V.} and Mane, {Rajaram S.}",

note = "Publisher Copyright: {\textcopyright} 2020 Elsevier B.V.",

year = "2020",

month = may,

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doi = "10.1016/j.mee.2020.111359",

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T1 - Electrodeposited spruce leaf-like structured copper bismuth oxide electrode for supercapacitor application

AU - AL-Osta, Ahmed

AU - Samer, Bushra Saleh

AU - Nakate, Umesh T.

AU - Jadhav, Vijaykumar V.

AU - Mane, Rajaram S.

PY - 2020/5/15

Y1 - 2020/5/15

N2 - Novel spruce leaf-like copper bismuth oxide (CuBi2O4) microstructured films have been deposited on stainless steel (SS) substrate by using a simple and cost-effective electrodeposition chemical route. The morphology of CuBi2O4 was studied using field emission scanning electron microscopy (FESEM) whereas X-ray diffraction (XRD) spectra recorded for phase confirmation. The spruce leaf-like architecture composed of nanoparticles was evidenced for the obtained CuBi2O4 material. The supercapacitor performance for prepared CuBi2O4 electrode calcined at 200, 300, 400, 500 °C temperatures were investigated. The cyclic-voltammetry and charge-discharge studies were carried out at different scan rates and current densities respectively. The highest specific capacitance 484 F/g was noted for CuBi2O4 electrode calcined at 500 °C at 10 mV/ s scan rate via cyclic-voltammetry analysis in 1 M NaOH electrolyte. The specific capacitance of 540.9 F/g was estimated from charge-discharge analysis at 10 mA/cm2 current density. The energy density of 146.8 Wh/Kg and power density 1555.5 W/Kg for optimized CuBi2O4 electrode at 10 mA/cm2 current density. The electrochemical impedance spectroscopy studies were also performed. The nanostructured CuBi2O4 material has exhibited supercapacitive properties for energy storage applications.

AB - Novel spruce leaf-like copper bismuth oxide (CuBi2O4) microstructured films have been deposited on stainless steel (SS) substrate by using a simple and cost-effective electrodeposition chemical route. The morphology of CuBi2O4 was studied using field emission scanning electron microscopy (FESEM) whereas X-ray diffraction (XRD) spectra recorded for phase confirmation. The spruce leaf-like architecture composed of nanoparticles was evidenced for the obtained CuBi2O4 material. The supercapacitor performance for prepared CuBi2O4 electrode calcined at 200, 300, 400, 500 °C temperatures were investigated. The cyclic-voltammetry and charge-discharge studies were carried out at different scan rates and current densities respectively. The highest specific capacitance 484 F/g was noted for CuBi2O4 electrode calcined at 500 °C at 10 mV/ s scan rate via cyclic-voltammetry analysis in 1 M NaOH electrolyte. The specific capacitance of 540.9 F/g was estimated from charge-discharge analysis at 10 mA/cm2 current density. The energy density of 146.8 Wh/Kg and power density 1555.5 W/Kg for optimized CuBi2O4 electrode at 10 mA/cm2 current density. The electrochemical impedance spectroscopy studies were also performed. The nanostructured CuBi2O4 material has exhibited supercapacitive properties for energy storage applications.

KW - Calcination effect

KW - Charge transport kinetics

KW - Copper bismuth oxide

KW - Electrochemical measurements

KW - Specific capacitance

KW - Spruce leaf-like nanostructure

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VL - 229

JO - Microelectronic Engineering

JF - Microelectronic Engineering

M1 - 111359

ER -

Electrodeposited spruce leaf-like structured copper bismuth oxide electrode for supercapacitor application

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Keywords

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