Structural evolution of metals at high temperature: Complementary investigations with neutron and synchrotron quantum beams

Klaus Dieter Liss

doi:10.1007/978-3-319-52392-7_87

Structural evolution of metals at high temperature: Complementary investigations with neutron and synchrotron quantum beams

Klaus Dieter Liss^*

^*Corresponding author for this work

Research output: Chapter in Book/Report/Conference proceeding › Conference contribution › peer-review

2 Scopus citations

Abstract

In situ neutron and synchrotron X-ray diffraction deliver unique and complementary insight into the microstructural evolution of metals at high temperature. Neutrons illuminate a larger bulk volume and reveal quantitative phase abundance, bulk texture, lattice parameter changes and other ensemble averaged quantities. In contrast, fine-bundled high-energy X-rays deliver reflections from a number of individual grains. For each constituting phase, their statistics and behavior in time reveal information about grain growth or refinement, subgrain formation, static and dynamic recovery and recrystallization, slip systems, twinning, etc. The complementarity between neutron and synchrotron radiation is demonstrated to study atomic order under ambient and extreme conditions. Examples are given on various metallic systems including magnesium, zirconium alloys and titanium aluminides.

Original language	English
Title of host publication	Magnesium Technology 2017
Editors	Neale R. Neelameggham, Alok Singh, Kiran N. Solanki, Dmytro Orlov
Publisher	Springer International Publishing
Pages	633-638
Number of pages	6
ISBN (Print)	9783319523910
DOIs	https://doi.org/10.1007/978-3-319-52392-7_87
State	Published - 2017
Externally published	Yes
Event	International Symposium on Magnesium Technology, 2017 - San Diego, United States Duration: 26 Feb 2017 → 2 Mar 2017

Publication series

Name	Minerals, Metals and Materials Series
Volume	Part F8
ISSN (Print)	2367-1181
ISSN (Electronic)	2367-1696

Conference

Conference	International Symposium on Magnesium Technology, 2017
Country	United States
City	San Diego
Period	26/02/17 → 2/03/17

Keywords

Grain reorientation
High pressure
High temperature
In situ studies
Magnesium
Materials oscilloscope
Metals
Phase transformation
Titanium aluminides
Zirconium

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Liss, K. D. (2017). Structural evolution of metals at high temperature: Complementary investigations with neutron and synchrotron quantum beams. In N. R. Neelameggham, A. Singh, K. N. Solanki, & D. Orlov (Eds.), Magnesium Technology 2017 (pp. 633-638). (Minerals, Metals and Materials Series; Vol. Part F8). Springer International Publishing. https://doi.org/10.1007/978-3-319-52392-7_87

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title = "Structural evolution of metals at high temperature: Complementary investigations with neutron and synchrotron quantum beams",

abstract = "In situ neutron and synchrotron X-ray diffraction deliver unique and complementary insight into the microstructural evolution of metals at high temperature. Neutrons illuminate a larger bulk volume and reveal quantitative phase abundance, bulk texture, lattice parameter changes and other ensemble averaged quantities. In contrast, fine-bundled high-energy X-rays deliver reflections from a number of individual grains. For each constituting phase, their statistics and behavior in time reveal information about grain growth or refinement, subgrain formation, static and dynamic recovery and recrystallization, slip systems, twinning, etc. The complementarity between neutron and synchrotron radiation is demonstrated to study atomic order under ambient and extreme conditions. Examples are given on various metallic systems including magnesium, zirconium alloys and titanium aluminides.",

keywords = "Grain reorientation, High pressure, High temperature, In situ studies, Magnesium, Materials oscilloscope, Metals, Phase transformation, Titanium aluminides, Zirconium",

author = "Liss, {Klaus Dieter}",

note = "Publisher Copyright: {\textcopyright} 2017, The Minerals, Metals & Materials Society. Copyright: Copyright 2018 Elsevier B.V., All rights reserved.; null ; Conference date: 26-02-2017 Through 02-03-2017",

year = "2017",

doi = "10.1007/978-3-319-52392-7_87",

language = "英语",

isbn = "9783319523910",

series = "Minerals, Metals and Materials Series",

publisher = "Springer International Publishing",

pages = "633--638",

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Liss, KD 2017, Structural evolution of metals at high temperature: Complementary investigations with neutron and synchrotron quantum beams. in NR Neelameggham, A Singh, KN Solanki & D Orlov (eds), Magnesium Technology 2017. Minerals, Metals and Materials Series, vol. Part F8, Springer International Publishing, pp. 633-638, International Symposium on Magnesium Technology, 2017, San Diego, United States, 26/02/17. https://doi.org/10.1007/978-3-319-52392-7_87

Structural evolution of metals at high temperature : Complementary investigations with neutron and synchrotron quantum beams. / Liss, Klaus Dieter.

Magnesium Technology 2017. ed. / Neale R. Neelameggham; Alok Singh; Kiran N. Solanki; Dmytro Orlov. Springer International Publishing, 2017. p. 633-638 (Minerals, Metals and Materials Series; Vol. Part F8).

Research output: Chapter in Book/Report/Conference proceeding › Conference contribution › peer-review

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AB - In situ neutron and synchrotron X-ray diffraction deliver unique and complementary insight into the microstructural evolution of metals at high temperature. Neutrons illuminate a larger bulk volume and reveal quantitative phase abundance, bulk texture, lattice parameter changes and other ensemble averaged quantities. In contrast, fine-bundled high-energy X-rays deliver reflections from a number of individual grains. For each constituting phase, their statistics and behavior in time reveal information about grain growth or refinement, subgrain formation, static and dynamic recovery and recrystallization, slip systems, twinning, etc. The complementarity between neutron and synchrotron radiation is demonstrated to study atomic order under ambient and extreme conditions. Examples are given on various metallic systems including magnesium, zirconium alloys and titanium aluminides.

KW - Grain reorientation

KW - High pressure

KW - High temperature

KW - In situ studies

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KW - Materials oscilloscope

KW - Metals

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KW - Zirconium

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