Influence of fluxing in the preparation of bulk Fe-based glassy alloys

C. Duhamel; K. G. Georgarakis; A. LeMoulec; A. R. Yavari; G. Vaughan; A. Baron; N. Lupu

doi:10.1016/j.jallcom.2008.08.132

Influence of fluxing in the preparation of bulk Fe-based glassy alloys

C. Duhamel, K. G. Georgarakis^*, A. LeMoulec, A. R. Yavari, G. Vaughan, A. Baron, N. Lupu

^*Corresponding author for this work

Research output: Contribution to journal › Article › peer-review

14 Scopus citations

Abstract

Fe-based master ingots, with composition [(Fe₅₀Co₅₀)₇₅B₂₀Si₅]₉₆Nb₄, have been prepared by arc-melting and subsequently purified using the fluxing technique. Rods, with diameters from 1 to 2.5 mm, ribbons and wires with a maximal diameter of 200 μm have been produced from these purified master ingots. The amorphous structure, thermal stability, hardness and magnetic properties of the specimens were studied. In particular, we show by high-energy synchrotron X-ray diffraction that the rods are fully amorphous up to a maximal diameter of 2 mm. Moreover, the [(Fe₅₀Co₅₀)₇₅B₂₀Si₅]₉₆Nb₄ glassy alloy exhibits high hardness (HV = 1050) combined with good soft-magnetic properties (H_c = 63 A/m).

Original language	English
Pages (from-to)	243-246
Number of pages	4
Journal	Journal of Alloys and Compounds
Volume	483
Issue number	1-2
DOIs	https://doi.org/10.1016/j.jallcom.2008.08.132
State	Published - 26 Aug 2009
Externally published	Yes

Keywords

Amorphous materials
Magnetic measurements
Synchrotron radiation
X-ray diffraction

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10.1016/j.jallcom.2008.08.132

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@article{77dd85831d05448e87069e64d96ebf61,

title = "Influence of fluxing in the preparation of bulk Fe-based glassy alloys",

abstract = "Fe-based master ingots, with composition [(Fe50Co50)75B20Si5]96Nb4, have been prepared by arc-melting and subsequently purified using the fluxing technique. Rods, with diameters from 1 to 2.5 mm, ribbons and wires with a maximal diameter of 200 μm have been produced from these purified master ingots. The amorphous structure, thermal stability, hardness and magnetic properties of the specimens were studied. In particular, we show by high-energy synchrotron X-ray diffraction that the rods are fully amorphous up to a maximal diameter of 2 mm. Moreover, the [(Fe50Co50)75B20Si5]96Nb4 glassy alloy exhibits high hardness (HV = 1050) combined with good soft-magnetic properties (Hc = 63 A/m).",

keywords = "Amorphous materials, Magnetic measurements, Synchrotron radiation, X-ray diffraction",

author = "C. Duhamel and Georgarakis, {K. G.} and A. LeMoulec and Yavari, {A. R.} and G. Vaughan and A. Baron and N. Lupu",

note = "Funding Information: Support from the French national project (ANR-BLAN-036 VMM ductiles) and the EU network “Ductile BMG Composites” coordinated by A.R.Y. are gratefully acknowledged.",

year = "2009",

month = aug,

day = "26",

doi = "10.1016/j.jallcom.2008.08.132",

language = "英语",

volume = "483",

pages = "243--246",

journal = "Journal of Alloys and Compounds",

issn = "0925-8388",

publisher = "Elsevier BV",

number = "1-2",

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TY - JOUR

T1 - Influence of fluxing in the preparation of bulk Fe-based glassy alloys

AU - Duhamel, C.

AU - Georgarakis, K. G.

AU - LeMoulec, A.

AU - Yavari, A. R.

AU - Vaughan, G.

AU - Baron, A.

AU - Lupu, N.

N1 - Funding Information: Support from the French national project (ANR-BLAN-036 VMM ductiles) and the EU network “Ductile BMG Composites” coordinated by A.R.Y. are gratefully acknowledged.

PY - 2009/8/26

Y1 - 2009/8/26

N2 - Fe-based master ingots, with composition [(Fe50Co50)75B20Si5]96Nb4, have been prepared by arc-melting and subsequently purified using the fluxing technique. Rods, with diameters from 1 to 2.5 mm, ribbons and wires with a maximal diameter of 200 μm have been produced from these purified master ingots. The amorphous structure, thermal stability, hardness and magnetic properties of the specimens were studied. In particular, we show by high-energy synchrotron X-ray diffraction that the rods are fully amorphous up to a maximal diameter of 2 mm. Moreover, the [(Fe50Co50)75B20Si5]96Nb4 glassy alloy exhibits high hardness (HV = 1050) combined with good soft-magnetic properties (Hc = 63 A/m).

AB - Fe-based master ingots, with composition [(Fe50Co50)75B20Si5]96Nb4, have been prepared by arc-melting and subsequently purified using the fluxing technique. Rods, with diameters from 1 to 2.5 mm, ribbons and wires with a maximal diameter of 200 μm have been produced from these purified master ingots. The amorphous structure, thermal stability, hardness and magnetic properties of the specimens were studied. In particular, we show by high-energy synchrotron X-ray diffraction that the rods are fully amorphous up to a maximal diameter of 2 mm. Moreover, the [(Fe50Co50)75B20Si5]96Nb4 glassy alloy exhibits high hardness (HV = 1050) combined with good soft-magnetic properties (Hc = 63 A/m).

KW - Amorphous materials

KW - Magnetic measurements

KW - Synchrotron radiation

KW - X-ray diffraction

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U2 - 10.1016/j.jallcom.2008.08.132

DO - 10.1016/j.jallcom.2008.08.132

M3 - 文章

AN - SCOPUS:69249235846

SN - 0925-8388

VL - 483

SP - 243

EP - 246

JO - Journal of Alloys and Compounds

JF - Journal of Alloys and Compounds

IS - 1-2

ER -

Influence of fluxing in the preparation of bulk Fe-based glassy alloys

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Keywords

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